TA Instruments

AR1756-0014f

15/03/2013 15:17:05

Sample name	ASW Blank coupon#20 + DI + beads 200rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	14 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:17:05

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 200.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	199.9	-563.21	10000	20.0	0.4612	0.992	-183.6	249.9	-0.7345	1879	168.5410	0.03008	210.68	21068	3.411E-3	0.0	0.0
2.0120	200.0	351.40	10000	20.0	0.4482	2.012	114.5	250.0	0.4582	1826	329.9600	0.02923	412.45	41245	3.411E-3	0.0	0.0
2.9920	200.0	357.55	10000	20.0	0.4460	2.992	116.5	250.0	0.4662	1817	576.8540	0.02908	721.07	72107	3.411E-3	0.0	0.0
3.9920	200.0	348.25	10000	20.0	0.4460	3.992	113.5	250.0	0.4541	1817	740.8440	0.02907	926.06	92606	3.411E-3	0.1	0.1
4.9920	200.0	347.73	10000	20.0	0.4458	4.992	113.3	250.0	0.4534	1816	984.3870	0.02906	1230.5	1.2305E5	3.411E-3	0.1	0.1
5.9920	200.0	344.11	10000	20.0	0.4470	5.992	112.2	250.0	0.4486	1821	1147.4900	0.02913	1434.4	1.4344E5	3.411E-3	0.1	0.1
6.9960	200.0	343.20	10000	20.0	0.4458	6.996	111.9	250.0	0.4475	1816	1392.4600	0.02906	1740.6	1.7406E5	3.411E-3	0.1	0.1
7.9920	200.0	340.44	10000	20.0	0.4435	7.992	111.0	250.0	0.4439	1807	1555.0300	0.02891	1943.8	1.9438E5	3.411E-3	0.1	0.1
9.0080	200.0	344.74	10000	20.0	0.4478	9.008	112.4	250.0	0.4495	1824	1801.3800	0.02920	2251.7	2.2517E5	3.411E-3	0.2	0.2
10.008	200.0	342.82	10000	20.0	0.4458	10.008	111.7	250.0	0.4470	1816	1963.3700	0.02906	2454.2	2.4542E5	3.411E-3	0.2	0.2
10.992	200.0	332.49	10000	20.0	0.4486	10.992	108.4	250.0	0.4334	1828	2126.7200	0.02924	2658.4	2.6584E5	3.411E-3	0.2	0.2
12.008	200.0	339.55	10000	20.0	0.4490	12.008	110.7	250.0	0.4427	1829	2371.7800	0.02927	2964.7	2.9647E5	3.411E-3	0.2	0.2
12.992	200.0	347.17	10000	20.0	0.4423	12.992	113.2	250.0	0.4527	1802	2536.6201	0.02883	3170.8	3.1708E5	3.411E-3	0.2	0.2
13.992	200.0	339.44	10000	20.0	0.4462	13.992	110.6	250.0	0.4426	1818	2780.1399	0.02908	3475.2	3.4752E5	3.411E-3	0.2	0.2
15.008	200.0	337.91	10000	20.0	0.4421	15.008	110.1	250.0	0.4406	1801	2943.5500	0.02882	3679.4	3.6794E5	3.411E-3	0.3	0.3
15.992	200.0	338.93	10000	20.0	0.4417	15.992	110.5	250.0	0.4419	1800	3188.6499	0.02879	3985.8	3.9858E5	3.411E-3	0.3	0.3
16.992	200.0	342.98	10000	20.0	0.4415	16.992	111.8	250.0	0.4472	1799	3351.8999	0.02878	4189.9	4.1899E5	3.411E-3	0.3	0.3
17.992	200.0	339.54	10000	20.0	0.4389	17.992	110.7	250.0	0.4427	1788	3598.4800	0.02861	4498.1	4.4981E5	3.411E-3	0.3	0.3
19.008	200.0	338.27	10000	20.0	0.4393	19.008	110.3	250.0	0.4410	1790	3763.3899	0.02864	4704.2	4.7042E5	3.411E-3	0.3	0.3
20.056	200.0	332.37	10000	20.0	0.4378	20.056	108.3	250.0	0.4333	1784	4006.0701	0.02854	5007.6	5.0076E5	3.411E-3	0.3	0.3
21.008	200.0	338.72	10000	20.0	0.4391	21.008	110.4	250.0	0.4416	1789	4169.4702	0.02862	5211.8	5.2118E5	3.411E-3	0.4	0.4
21.992	200.0	332.44	10000	20.0	0.4372	21.992	108.4	250.0	0.4334	1781	4332.0298	0.02850	5415.0	5.4150E5	3.411E-3	0.4	0.4
22.992	200.0	331.38	10000	20.0	0.4411	22.992	108.0	250.0	0.4320	1797	4577.1401	0.02875	5721.4	5.7214E5	3.411E-3	0.4	0.4
23.992	200.0	335.04	10000	20.0	0.4415	23.992	109.2	250.0	0.4368	1799	4741.4102	0.02878	5926.8	5.9268E5	3.411E-3	0.4	0.4
24.992	200.0	341.22	10000	20.0	0.4435	24.992	111.2	250.0	0.4449	1807	4985.3701	0.02891	6231.7	6.2317E5	3.411E-3	0.4	0.4
25.992	200.0	341.96	10000	20.0	0.4417	25.992	111.5	250.0	0.4459	1800	5148.7002	0.02880	6435.9	6.4359E5	3.411E-3	0.4	0.4
27.008	200.0	336.66	10000	20.0	0.4466	27.008	109.7	250.0	0.4389	1819	5393.7598	0.02911	6742.2	6.7422E5	3.411E-3	0.5	0.5
27.992	200.0	340.51	10000	20.0	0.4431	27.992	111.0	250.0	0.4440	1805	5558.0801	0.02889	6947.6	6.9476E5	3.411E-3	0.5	0.5
28.996	200.0	341.68	10000	20.0	0.4431	28.996	111.4	250.0	0.4455	1805	5803.0601	0.02889	7253.8	7.2538E5	3.411E-3	0.5	0.5
30.008	200.0	337.86	10000	20.0	0.4462	30.008	110.1	250.0	0.4405	1818	5968.0298	0.02909	7460.0	7.4600E5	3.411E-3	0.5	0.5
31.008	200.0	343.74	10000	20.0	0.4407	31.008	112.0	250.0	0.4482	1795	6128.9800	0.02873	7661.2	7.6612E5	3.411E-3	0.5	0.5
32.008	200.0	337.91	10000	20.0	0.4378	32.008	110.1	250.0	0.4405	1784	6374.7598	0.02854	7968.5	7.9685E5	3.411E-3	0.5	0.5
33.008	200.0	333.31	10000	20.0	0.4397	33.008	108.6	250.0	0.4345	1791	6537.2402	0.02866	8171.6	8.1716E5	3.411E-3	0.6	0.6
34.008	200.0	338.81	10000	20.0	0.4376	34.008	110.4	250.0	0.4417	1783	6782.3599	0.02853	8478.0	8.4780E5	3.411E-3	0.6	0.6
35.008	200.0	337.37	10000	20.0	0.4429	35.008	110.0	250.0	0.4399	1805	6945.6401	0.02887	8682.1	8.6821E5	3.411E-3	0.6	0.6
35.996	200.0	339.07	10000	20.0	0.4387	35.996	110.5	250.0	0.4421	1787	7190.6401	0.02860	8988.3	8.9883E5	3.411E-3	0.6	0.6
37.008	200.0	336.83	10000	20.0	0.4470	37.008	109.8	250.0	0.4392	1821	7354.1299	0.02914	9192.7	9.1927E5	3.411E-3	0.6	0.6
37.992	200.0	336.96	10000	20.0	0.4393	37.992	109.8	250.0	0.4394	1790	7600.4399	0.02864	9500.6	9.5006E5	3.411E-3	0.6	0.6
38.992	200.0	329.17	10000	20.0	0.4443	38.992	107.3	250.0	0.4291	1810	7765.4800	0.02896	9706.9	9.7069E5	3.411E-3	0.6	0.6
39.992	200.0	332.32	10000	20.0	0.4447	39.992	108.3	250.0	0.4332	1812	7927.3398	0.02899	9909.2	9.9092E5	3.411E-3	0.7	0.7
41.008	200.0	341.96	10000	20.0	0.4413	41.008	111.5	250.0	0.4459	1798	8171.6602	0.02877	10215	1.0215E6	3.411E-3	0.7	0.7
42.012	200.0	331.70	10000	20.0	0.4433	42.012	108.1	250.0	0.4324	1806	8334.2500	0.02890	10418	1.0418E6	3.411E-3	0.7	0.7
43.008	200.0	341.21	10000	20.0	0.4403	43.008	111.2	250.0	0.4449	1794	8579.3496	0.02870	10724	1.0724E6	3.411E-3	0.7	0.7
44.008	200.0	338.21	10000	20.0	0.4346	44.008	110.2	250.0	0.4410	1771	8742.5703	0.02833	10928	1.0928E6	3.411E-3	0.7	0.7
44.992	200.0	337.42	10000	20.0	0.4378	44.992	110.0	250.0	0.4399	1784	8987.6104	0.02854	11235	1.1235E6	3.411E-3	0.7	0.7
45.992	200.0	342.22	10000	20.0	0.4366	45.992	111.5	250.0	0.4462	1779	9151.0000	0.02847	11439	1.1439E6	3.411E-3	0.8	0.8
47.012	200.0	334.89	10000	20.0	0.4362	47.012	109.2	250.0	0.4366	1777	9396.0498	0.02843	11745	1.1745E6	3.411E-3	0.8	0.8
47.992	200.0	337.79	10000	20.0	0.4380	47.992	110.1	250.0	0.4404	1785	9559.5996	0.02856	11950	1.1950E6	3.411E-3	0.8	0.8
48.992	200.0	344.02	10000	20.0	0.4370	48.992	112.1	250.0	0.4485	1781	9722.6904	0.02849	12153	1.2153E6	3.411E-3	0.8	0.8
49.992	200.0	338.85	10000	20.0	0.4405	49.992	110.4	250.0	0.4418	1795	9968.9902	0.02871	12461	1.2461E6	3.411E-3	0.8	0.8
51.008	200.0	343.81	10000	20.0	0.4350	51.008	112.1	250.0	0.4482	1772	10131.000	0.02835	12664	1.2664E6	3.411E-3	0.9	0.9
51.992	200.0	335.05	10000	20.0	0.4389	51.992	109.2	250.0	0.4368	1788	10376.100	0.02861	12970	1.2970E6	3.411E-3	0.9	0.9
52.992	200.0	337.40	10000	20.0	0.4380	52.992	110.0	250.0	0.4399	1785	10539.500	0.02856	13174	1.3174E6	3.411E-3	0.9	0.9
53.992	200.0	336.72	10000	20.0	0.4384	53.992	109.8	250.0	0.4390	1786	10785.300	0.02858	13482	1.3482E6	3.411E-3	0.9	0.9
55.008	200.0	330.78	10000	20.0	0.4372	55.008	107.8	250.0	0.4313	1781	10947.800	0.02850	13685	1.3685E6	3.411E-3	0.9	0.9
55.992	200.0	340.95	10000	20.0	0.4393	55.992	111.1	250.0	0.4445	1790	11193.800	0.02864	13992	1.3992E6	3.411E-3	0.9	0.9
57.008	200.0	338.50	10000	20.0	0.4403	57.008	110.3	250.0	0.4414	1794	11356.300	0.02870	14195	1.4195E6	3.411E-3	1.0	1.0
58.008	200.0	336.40	10000	20.0	0.4403	58.008	109.6	250.0	0.4386	1794	11603.400	0.02870	14504	1.4504E6	3.411E-3	1.0	1.0
58.996	200.0	337.72	10000	20.0	0.4374	58.996	110.1	250.0	0.4403	1782	11764.900	0.02851	14706	1.4706E6	3.411E-3	1.0	1.0
59.992	200.0	342.79	10000	20.0	0.4382	59.992	111.7	250.0	0.4469	1786	11928.000	0.02857	14910	1.4910E6	3.411E-3	1.0	1.0

